3MWK
Q28E mutant of HERA N-terminal RecA-like domain, complex with 8-oxo-AMP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2010-04-23 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 91.916, 91.916, 108.006 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.960 - 1.450 |
R-factor | 0.16105 |
Rwork | 0.159 |
R-free | 0.20914 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2gxs |
RMSD bond length | 0.022 |
RMSD bond angle | 1.981 |
Data reduction software | XDS |
Data scaling software | SADABS |
Phasing software | PHASER |
Refinement software | REFMAC (5.6.0070) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.600 | 1.480 |
High resolution limit [Å] | 1.450 | 1.450 |
Rmerge | 0.019 | 0.596 |
Number of reflections | 82310 | |
<I/σ(I)> | 15.7 | 1.4 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 15.2 | 14.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | VAPOR DIFFUSION, SITTING DROP |