3MQS
Crystal Structure of the USP7:Hdm2(PSTS) complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.54 |
Spacegroup name | P 41 |
Unit cell lengths | 69.840, 69.840, 45.770 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.800 - 2.400 |
R-factor | 0.214 |
Rwork | 0.214 |
R-free | 0.25500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1yy6 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.300 |
Data reduction software | CrystalClear |
Data scaling software | CrystalClear |
Phasing software | CNS |
Refinement software | CNS (1.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.800 | 2.490 |
High resolution limit [Å] | 2.400 | 2.400 |
Number of reflections | 8727 | |
<I/σ(I)> | 5.9 | 2.6 |
Redundancy | 4.5 | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293 | 30% PEG4000, 0.2M Lithium Sulfate, 0.1M Tris, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |