3MQ1
Crystal Structure of Dust Mite Allergen Der p 5
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-05-08 |
Detector | RIGAKU SATURN 92 |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 46.780, 96.570, 167.890 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.598 - 2.800 |
R-factor | 0.2287 |
Rwork | 0.226 |
R-free | 0.27890 |
RMSD bond length | 0.001 |
RMSD bond angle | 0.307 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.5_2)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Number of reflections | 19292 | |
<I/σ(I)> | 15.7 | 2.5 |
Completeness [%] | 98.8 | 98.5 |
Redundancy | 6.4 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.2 | 294 | 31.5% MPD, 90 mM Na/K phosphate, pH 6.2, VAPOR DIFFUSION, SITTING DROP, temperature 294K |