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3MKV

Crystal structure of amidohydrolase eaj56179

Replaces:  2R8C
Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 31-ID
Synchrotron siteAPS
Beamline31-ID
Temperature [K]100
Detector technologyCCD
Collection date2006-06-25
DetectorMAR CCD 165 mm
Spacegroup nameP 1 21 1
Unit cell lengths92.022, 198.599, 104.294
Unit cell angles90.00, 107.76, 90.00
Refinement procedure
Resolution40.000 - 2.400
R-factor0.17306
Rwork0.171
R-free0.22860
Structure solution methodSAD
RMSD bond length0.006
RMSD bond angle0.986
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareSHELX
Refinement softwareREFMAC (5.3.0034)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.490
High resolution limit [Å]2.4002.400
Rmerge0.0900.880
Number of reflections140169
<I/σ(I)>5.60.8
Completeness [%]92.685.2
Redundancy2.52.2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP7.522% PEG 8000 PH 7.5, 0.1M AMMONIUM SULFATE, 10% GLYCEROL, VAPOR DIFFUSION, SITTING DROP, TEMPERATURE 294K

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