3MIU
Structure of Banana Lectin-pentamannose complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2005-08-08 |
Detector | MARRESEARCH |
Wavelength(s) | 1.54 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 80.911, 80.911, 147.405 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 24.920 - 2.630 |
R-factor | 0.21875 |
Rwork | 0.217 |
R-free | 0.24335 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1x1v |
RMSD bond length | 0.009 |
RMSD bond angle | 1.279 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.720 |
High resolution limit [Å] | 2.630 | 2.630 |
Rmerge | 0.066 | 0.428 |
Number of reflections | 17137 | |
<I/σ(I)> | 33 | 4.9 |
Completeness [%] | 99.7 | 98.7 |
Redundancy | 8.76 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 298 | ZINC ACETATE DIHYDRATE, SODIUM CACODYLATE, 1,6-HEXANEDIOL, pH 8.0, VAPOR DIFFUSION, SITTING DROP, temperature 298K |