3MC3
Crystal structure of DsrE/DsrF-like family protein (NP_342589.1) from SULFOLOBUS SOLFATARICUS at 1.49 A resolution
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL11-1 |
Synchrotron site | SSRL |
Beamline | BL11-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-11-15 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 0.91837,0.97871,0.97831 |
Spacegroup name | H 3 |
Unit cell lengths | 64.070, 64.070, 105.680 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 26.832 - 1.490 |
R-factor | 0.123 |
Rwork | 0.122 |
R-free | 0.14000 |
Structure solution method | MAD |
RMSD bond length | 0.017 |
RMSD bond angle | 1.509 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELX |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 26.832 | 26.832 | 1.540 |
High resolution limit [Å] | 1.490 | 3.210 | 1.490 |
Rmerge | 0.030 | 0.017 | 0.315 |
Number of reflections | 26406 | 5154 | 4712 |
<I/σ(I)> | 13.48 | 34.9 | 2 |
Completeness [%] | 96.1 | 97.4 | 94.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 277 | 5.0000% polyethylene glycol 3000, 40.0000% polyethylene glycol 400, 0.1M MES pH 6.0, NANODROP', VAPOR DIFFUSION, SITTING DROP, temperature 277K |