Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X4A |
Synchrotron site | NSLS |
Beamline | X4A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-04-06 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.97915 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 69.788, 63.687, 104.765 |
Unit cell angles | 90.00, 98.85, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.000 |
R-factor | 0.18218 |
Rwork | 0.181 |
R-free | 0.21080 |
Structure solution method | SAD |
RMSD bond length | 0.014 |
RMSD bond angle | 1.375 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.000 |
Rmerge | 0.067 |
Number of reflections | 56682 |
Completeness [%] | 97.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | 19% PEG 3350, 0.1M Bis-Tris, 0.2M Lithium sulfate, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 293.0K |