3M7A
Crystal structure of Saro_0823 (YP_496102.1) a protein of unknown function from NOVOSPHINGOBIUM AROMATICIVORANS DSM 12444 at 1.22 A resolution
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL11-1 |
Synchrotron site | SSRL |
Beamline | BL11-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-12-02 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 0.97883,0.91837 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 81.401, 65.190, 59.730 |
Unit cell angles | 90.00, 128.60, 90.00 |
Refinement procedure
Resolution | 45.531 - 1.220 |
R-factor | 0.119 |
Rwork | 0.117 |
R-free | 0.14800 |
Structure solution method | MAD |
RMSD bond length | 0.012 |
RMSD bond angle | 1.537 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELX |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 45.531 | 45.531 | 1.260 |
High resolution limit [Å] | 1.220 | 2.630 | 1.220 |
Rmerge | 0.090 | 0.052 | 0.658 |
Number of reflections | 71683 | 7353 | 6473 |
<I/σ(I)> | 10.24 | 29.8 | 1.8 |
Completeness [%] | 98.6 | 99.1 | 97.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.86 | 277 | 29.5000% polyethylene glycol 4000, 0.2000M magnesium chloride, 0.1M TRIS pH 8.86, NANODROP', VAPOR DIFFUSION, SITTING DROP, temperature 277K |