3LYN
STRUCTURE OF GREEN ABALONE LYSIN DIMER
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-1 |
Synchrotron site | SSRL |
Beamline | BL9-1 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1998-05-01 |
Detector | MARRESEARCH |
Spacegroup name | P 61 |
Unit cell lengths | 119.170, 119.170, 51.290 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 100.000 - 1.700 |
R-factor | 0.215 * |
R-free | 0.25900 * |
Structure solution method | MIR |
RMSD bond length | 0.009 |
RMSD bond angle | 1.890 * |
Data reduction software | MOSFLM |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | SOLVE |
Refinement software | SHELXL |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.700 | 1.750 |
High resolution limit [Å] | 1.710 | 1.710 |
Rmerge | 0.051 * | 0.387 * |
Number of reflections | 44479 | |
<I/σ(I)> | 9.7 | 1.9 |
Completeness [%] | 97.8 | 92.1 |
Redundancy | 4.4 | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4 | 1.26 M AMMONIUM SULFATE 0.10 M SODIUM ACETATE 0.20 M SODIUM CHLORIDE, pH 4.0 |