3LWX
Crystal structure of Na(+)-translocating NADH-quinone reductase subunit C (YP_001302508.1) from Parabacteroides distasonis ATCC 8503 at 1.10 A resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-01-25 |
Detector | MARMOSAIC 325 mm CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 37.444, 60.693, 82.758 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.739 - 1.100 |
R-factor | 0.117 |
Rwork | 0.116 |
R-free | 0.13800 |
Structure solution method | SAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.474 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELX |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 29.739 | 29.739 | 1.140 |
High resolution limit [Å] | 1.100 | 2.370 | 1.100 |
Rmerge | 0.041 | 0.025 | 0.534 |
Number of reflections | 74185 | 14688 | 13515 |
<I/σ(I)> | 14.69 | 50.9 | 2.2 |
Completeness [%] | 95.2 | 99.1 | 89.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 277 | 15.0000% Glycerol, 0.1700M NaOAc, 25.5000% PEG-4000, 0.1M TRIS pH 8.5, NANODROP, VAPOR DIFFUSION, SITTING DROP, temperature 277K |