3LWF
Crystal structure of Putative transcriptional regulator (NP_470886.1) from LISTERIA INNOCUA at 2.06 A resolution
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL11-1 |
Synchrotron site | SSRL |
Beamline | BL11-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-12-03 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 0.97925,0.91837,0.97898 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 108.961, 115.782, 75.927 |
Unit cell angles | 90.00, 120.70, 90.00 |
Refinement procedure
Resolution | 72.830 - 2.060 |
R-factor | 0.182 |
Rwork | 0.180 |
R-free | 0.21800 |
Structure solution method | MAD |
RMSD bond length | 0.015 |
RMSD bond angle | 1.446 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELX |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 72.830 | 72.830 | 2.130 |
High resolution limit [Å] | 2.060 | 4.420 | 2.060 |
Rmerge | 0.083 | 0.039 | 0.639 |
Number of reflections | 49880 | 5087 | 4716 |
<I/σ(I)> | 10.62 | 28.7 | 2 |
Completeness [%] | 99.4 | 98.4 | 99.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 10.3 | 293 | 1.9500M ammonium sulfate, 0.2000M lithium sulfate, 0.1M CAPS pH 10.3, NANODROP, VAPOR DIFFUSION, SITTING DROP, temperature 293K |