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3LUF

Structure of probable two-component system response regulator/GGDEF domain protein

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSLS BEAMLINE X29A
Synchrotron siteNSLS
BeamlineX29A
Temperature [K]100
Detector technologyCCD
Collection date2009-11-19
DetectorADSC QUANTUM 315
Wavelength(s)0.9793
Spacegroup nameP 1
Unit cell lengths41.195, 53.699, 57.887
Unit cell angles75.39, 80.99, 77.41
Refinement procedure
Resolution40.000 - 1.760
R-factor0.189
Rwork0.187
R-free0.22600
Structure solution methodSAD
RMSD bond length0.014
RMSD bond angle1.498
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareSHELXD
Refinement softwareREFMAC
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]40.0001.790
High resolution limit [Å]1.7601.760
Rmerge0.0630.216
Number of reflections44744
<I/σ(I)>56.36.9
Completeness [%]97.495.4
Redundancy3.93.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP5.52980.1 M Bis-Tris pH 5.5, 25% PEG 3350, 0.2M MgCl2, Vapor diffusion, Sitting drop, temperature 298K

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