3LSU
Crystal Structure of SOD2 from Saccharomyces cerevisiae
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ DW |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2009-04-23 |
Detector | RIGAKU RAXIS HTC |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 |
Unit cell lengths | 63.657, 64.933, 66.550 |
Unit cell angles | 109.36, 106.35, 109.68 |
Refinement procedure
Resolution | 32.376 - 1.896 |
R-factor | 0.163 |
Rwork | 0.162 |
R-free | 0.19500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1qnm |
RMSD bond length | 0.007 |
RMSD bond angle | 1.045 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER (1.3.2) |
Refinement software | PHENIX (1.5_2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 80.000 | 1.970 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.083 | 0.314 |
Number of reflections | 59997 | |
<I/σ(I)> | 14.8 | 3.7 |
Completeness [%] | 89.5 | 53.1 |
Redundancy | 3.3 | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 277 | 0.2M sodium malonate, 20% PEG 3350, pH 7.0, vapor diffusion, hanging drop, temperature 277K |