3LQZ

Crystal Structure of HLA-DP2

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 8.2.2
Synchrotron site	ALS
Beamline	8.2.2
Temperature [K]	170
Detector technology	CCD
Detector	ADSC QUANTUM 315
Wavelength(s)	1.0
Spacegroup name	P 31 2 1
Unit cell lengths	157.282, 157.282, 61.805
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	50.000 - 3.250
R-factor	0.21865
Rwork	0.217
R-free	0.25094
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.012
RMSD bond angle	1.490
Data reduction software	HKL-2000
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	REFMAC (5.3.0040)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	136.080	3.283
High resolution limit [Å]	3.250	3.250
Number of reflections	12053
Completeness [%]	100.0	89.1
Redundancy	7.1	6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7.5	293	20% PEG4000, 300mM Sodium Chloride, HEPES, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K
1	VAPOR DIFFUSION, HANGING DROP	7.5	293	20% PEG4000, 300mM Sodium Chloride, HEPES, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K