3LQV
Branch Recognition by SF3b14
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-01-01 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.11586 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 101.848, 112.702, 82.163 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.470 - 2.380 |
R-factor | 0.216 |
Rwork | 0.214 |
R-free | 0.25800 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.016 |
RMSD bond angle | 1.551 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | REFMAC (5.2.0005) |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.490 |
High resolution limit [Å] | 2.380 | 5.170 | 2.380 |
Rmerge | 0.055 | 0.024 | 0.301 |
Number of reflections | 18348 | ||
<I/σ(I)> | 15.3 | ||
Completeness [%] | 95.9 | 99.6 | 84 |
Redundancy | 3.8 | 3.9 | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | 298 | PEG3350, 0.2M NaCl, 20mM Adenine, pH 6, vapor diffusion, temperature 298K |