3LMZ
Crystal structure of Putative sugar isomerase. (YP_001305105.1) from Parabacteroides distasonis ATCC 8503 at 1.44 A resolution
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-11-06 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 0.91162,0.97944,0.97932 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 78.594, 81.906, 95.485 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.355 - 1.440 |
R-factor | 0.151 |
Rwork | 0.149 |
R-free | 0.18500 |
Structure solution method | MAD |
RMSD bond length | 0.018 |
RMSD bond angle | 1.688 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 28.355 | 28.355 | 1.490 |
High resolution limit [Å] | 1.440 | 3.100 | 1.440 |
Rmerge | 0.053 | 0.030 | 0.490 |
Number of reflections | 47272 | 7549 | 8307 |
<I/σ(I)> | 10.02 | 28.2 | 1.8 |
Completeness [%] | 76.7 | 69.7 | 79 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.57 | 277 | 19.5000% polyethylene glycol 3000, 0.1M citric acid pH 5.57, NANODROP, VAPOR DIFFUSION, SITTING DROP, temperature 277K |