3LJ8
Crystal Structure of MKP-4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-5A |
Synchrotron site | Photon Factory |
Beamline | BL-5A |
Temperature [K] | 93 |
Detector technology | CCD |
Collection date | 2005-05-21 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 91.926, 91.926, 56.605 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 35.680 - 2.700 |
R-factor | 0.241 |
Rwork | 0.238 |
R-free | 0.30400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1zzw |
RMSD bond length | 0.008 |
RMSD bond angle | 1.580 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | CNS (0.9) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.850 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.032 | 0.228 |
Number of reflections | 7730 | |
<I/σ(I)> | 14.7 | 3.4 |
Completeness [%] | 98.3 | 98.5 |
Redundancy | 5.7 | 6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 291 | 10% ethanol, 1.3M NaCl, 0.2M MgSO4, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K |