3LIU
Crystal structure of Putative cell adhesion protein (YP_001304840.1) from Parabacteroides distasonis ATCC 8503 at 2.05 A resolution
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-11-05 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 0.91837,0.97939,0.97922 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 64.372, 101.934, 130.891 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.493 - 2.050 |
R-factor | 0.173 |
Rwork | 0.170 |
R-free | 0.21900 |
Structure solution method | MAD |
RMSD bond length | 0.016 |
RMSD bond angle | 1.512 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELX |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 47.493 | 47.493 | 2.120 |
High resolution limit [Å] | 2.050 | 4.400 | 2.050 |
Rmerge | 0.108 | 0.034 | 0.729 |
Number of reflections | 54734 | 5801 | 5160 |
<I/σ(I)> | 10.91 | 29.9 | 2.1 |
Completeness [%] | 99.7 | 98.7 | 99.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4 | 277 | 0.1600M ammonium sulfate, 20.1000% polyethylene glycol 4000, 20.0000% Glycerol, 0.1M sodium acetate pH 4.0, NANODROP', VAPOR DIFFUSION, SITTING DROP, temperature 277K |