3LH9
Crystal structure of mouse VPS26B(L197S/R199E) in spacegroup P41 21 2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-11-27 |
Wavelength(s) | 0.95364 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 118.350, 118.350, 214.513 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.541 - 2.400 |
R-factor | 0.2001 |
Rwork | 0.199 |
R-free | 0.22790 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2r51 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.169 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.5_2)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.200 | 2.530 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.067 | 0.552 |
Number of reflections | 60249 | |
<I/σ(I)> | 24.1 | 3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 8.6 | 6.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 289 | 2M sodium formate, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 289K |