3LG7
Crystal structure of HIV epitope-scaffold 4E10_S0_1EZ3A_002_C
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 107 |
Detector technology | CCD |
Collection date | 2008-05-09 |
Detector | RIGAKU SATURN 944+ |
Wavelength(s) | 1.54 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 91.600, 94.870, 108.390 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.820 - 2.500 |
R-factor | 0.25923 |
Rwork | 0.257 |
R-free | 0.30121 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | Computationally-derived model of the epitope-scaffold based on 1EZ3 |
RMSD bond length | 0.014 |
RMSD bond angle | 1.189 |
Data reduction software | CrystalClear |
Data scaling software | CrystalClear |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.820 | 2.590 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.107 | 0.429 |
Number of reflections | 33220 | |
<I/σ(I)> | 6.6 | 2 |
Completeness [%] | 99.5 | 96.8 |
Redundancy | 4.53 | 3.78 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 277 | Ammonium sulfate, bis Tris, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |