3LFR
The Crystal Structure of a CBS Domain from a Putative Metal Ion Transporter Bound to AMP from Pseudomonas syringae to 1.55A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-08-12 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9794 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 47.150, 50.650, 51.867 |
Unit cell angles | 90.00, 112.26, 90.00 |
Refinement procedure
Resolution | 34.840 - 1.530 |
R-factor | 0.177 |
Rwork | 0.175 |
R-free | 0.21200 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.481 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | HKL-3000 |
Refinement software | REFMAC (refmac_5.5.0102) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.610 |
High resolution limit [Å] | 1.530 | 3.340 | 1.550 |
Rmerge | 0.102 | 0.073 | 0.652 |
Number of reflections | 33409 | ||
<I/σ(I)> | 13.3 | ||
Completeness [%] | 99.2 | 94.7 | 99.7 |
Redundancy | 3.1 | 3.1 | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 289 | 25% PEG 3350, 0.1M Hepes PH 7.5, 0.2M Lithium sulfate, VAPOR DIFFUSION, SITTING DROP, temperature 289K |