3L9U
Crystal Structure of Salmonella enterica serovar Typhimurium DsbL
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-08-15 |
Detector | ADSC QUANTUM 210r |
Wavelength(s) | 0.956667 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 85.582, 46.593, 60.222 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.404 - 1.568 |
R-factor | 0.152 |
Rwork | 0.150 |
R-free | 0.18400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3c7m |
RMSD bond length | 0.006 |
RMSD bond angle | 0.944 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.5_2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.600 |
High resolution limit [Å] | 1.568 | 1.570 |
Rmerge | 0.066 | 0.459 |
Number of reflections | 34491 | |
<I/σ(I)> | 10.6 | 4.12 |
Completeness [%] | 99.9 | 100 |
Redundancy | 7.2 | 7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.2 | 293 | 2.6-3.4 M sodium malonate pH 7.0 -7.4, VAPOR DIFFUSION, HANGING DROP, temperature 293K |