3L7B
Crystal Structure of Glycogen Phosphorylase DK3 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X13 |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | X13 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-07-29 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 0.81 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 129.113, 129.113, 116.956 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 86.710 - 2.000 |
R-factor | 0.189 |
Rwork | 0.188 |
R-free | 0.21500 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 2prj |
RMSD bond length | 0.010 |
RMSD bond angle | 1.168 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | REFMAC |
Refinement software | REFMAC (5.3.0037) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 99.000 | 99.000 | 2.030 |
High resolution limit [Å] | 2.000 | 5.430 | 2.000 |
Rmerge | 0.071 | 0.046 | 0.487 |
Number of reflections | 66691 | ||
<I/σ(I)> | 16.1 | ||
Completeness [%] | 99.2 | 98.5 | 98.8 |
Redundancy | 8 | 7.2 | 8.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | SMALL TUBES | 6.7 | 289 | 10MM BES BUFFER, 3MM DDT, pH 6.7, small tubes, temperature 289K |