3L09
Crystal structure of Putative transcriptional regulator (JANN_22DEC04_CONTIG27_REVISED_GENE3569) from Jannaschia sp. CCS1 at 2.81 A resolution
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-03-16 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 0.97939,0.91162,0.97925 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 69.953, 81.722, 199.921 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.932 - 2.810 |
R-factor | 0.202 |
Rwork | 0.199 |
R-free | 0.24500 |
Structure solution method | MAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.120 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELX |
Refinement software | BUSTER (2.8.0) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 46.932 | 46.932 | 2.910 |
High resolution limit [Å] | 2.810 | 6.000 | 2.810 |
Rmerge | 0.124 | 0.046 | 0.757 |
Number of reflections | 28370 | 3097 | 2581 |
<I/σ(I)> | 8.29 | 17.9 | 2.3 |
Completeness [%] | 98.5 | 97.5 | 91 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 20.0000% polyethylene glycol 3350, 0.2500M lithium sulfate, NANODROP, VAPOR DIFFUSION, SITTING DROP, temperature 293K |