3KXL
crystal structure of SsGBP mutation variant G235S
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Collection date | 2009-10-26 |
Wavelength(s) | 1.0000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 55.608, 71.136, 97.112 |
Unit cell angles | 90.00, 96.98, 90.00 |
Refinement procedure
Resolution | 38.372 - 2.500 |
R-factor | 0.241 |
Rwork | 0.240 |
R-free | 0.26400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2qtf |
RMSD bond length | 0.002 |
RMSD bond angle | 0.405 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.5_2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.570 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.069 | 0.364 |
Number of reflections | 26261 | |
<I/σ(I)> | 8.7 | 3.8 |
Completeness [%] | 99.8 | 99.6 |
Redundancy | 3.9 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289 | 12% (w/v) PEG 3350, 0.16M sodium thiocyanate, VAPOR DIFFUSION, HANGING DROP, temperature 289K |