3KXK
Crystal structure of SsGBP mutation variant G235P
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Detector technology | IMAGE PLATE |
Collection date | 2009-08-02 |
Detector | RIGAKU RAXIS |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 55.710, 71.239, 97.672 |
Unit cell angles | 90.00, 96.81, 90.00 |
Refinement procedure
Resolution | 38.819 - 2.350 |
R-factor | 0.245 |
Rwork | 0.244 |
R-free | 0.26600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2qtf |
RMSD bond length | 0.002 |
RMSD bond angle | 0.431 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.5_2) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.430 |
High resolution limit [Å] | 2.350 | 5.060 | 2.350 |
Rmerge | 0.051 | 0.023 | 0.408 |
Number of reflections | 31222 | ||
<I/σ(I)> | 13.2 | ||
Completeness [%] | 98.4 | 99.1 | 97.2 |
Redundancy | 4 | 3.9 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289 | 12% (w/v) PEG 3350, 0.18M sodium thiocyanate, VAPOR DIFFUSION, HANGING DROP, temperature 289K |