3KXI
crystal structure of SsGBP and GDP complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Collection date | 2009-03-16 |
Wavelength(s) | 1.54178 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 67.322, 68.471, 92.148 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 23.227 - 2.650 |
R-factor | 0.227 |
Rwork | 0.224 |
R-free | 0.29000 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.828 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.5_2) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.740 |
High resolution limit [Å] | 2.650 | 5.710 | 2.650 |
Rmerge | 0.079 | 0.049 | 0.374 |
Number of reflections | 11840 | ||
<I/σ(I)> | 14.2 | ||
Completeness [%] | 91.6 | 81.3 | 87.9 |
Redundancy | 2.7 | 2.6 | 2.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289 | 10% (w/v) PEG 3350, 0.18M sodium thiocyanate, VAPOR DIFFUSION, HANGING DROP, temperature 289K |