3KXD
Crystal structure of the mthk rck in complex with cadmium
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-1 |
Synchrotron site | SSRL |
Beamline | BL9-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-03-05 |
Detector | ADSC QUANTUM 315 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 58.022, 38.293, 96.634 |
Unit cell angles | 90.00, 95.10, 90.00 |
Refinement procedure
Resolution | 57.830 - 2.200 |
R-factor | 0.1878 |
Rwork | 0.184 |
R-free | 0.25364 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 2aej |
RMSD bond length | 0.021 |
RMSD bond angle | 1.877 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | REFMAC |
Refinement software | REFMAC |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 57.830 |
High resolution limit [Å] | 2.200 |
Rmerge | 0.039 |
Number of reflections | 21805 |
<I/σ(I)> | 10.8 |
Completeness [%] | 99.4 |
Redundancy | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.7 | 318 | 1M NH4-FORMATE, 10% PEG 4000, 0.1M NA ACETATE, PH 4.7, VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 318K |