3KU0
Structure of GAP31 with adenine at its binding pocket
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X12B |
Synchrotron site | NSLS |
Beamline | X12B |
Temperature [K] | 125 |
Detector technology | CCD |
Collection date | 2003-10-01 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 48.373, 44.395, 137.270 |
Unit cell angles | 90.00, 98.38, 90.00 |
Refinement procedure
Resolution | 47.350 - 1.900 |
R-factor | 0.2 |
Rwork | 0.200 |
R-free | 0.24200 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.300 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | CNS |
Refinement software | CNS (1.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.350 | 2.020 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.041 | |
Number of reflections | 46674 | |
Completeness [%] | 96.4 | 71 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 300 | 100 mM Tris-HCl, pH 8.5, 2.0 M ammonium sulfate, VAPOR DIFFUSION, HANGING DROP, temperature 300K |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 300 | 100 mM Tris-HCl, pH 8.5, 2.0 M ammonium sulfate, VAPOR DIFFUSION, HANGING DROP, temperature 300K |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 300 | 100 mM Tris-HCl, pH 8.5, 2.0 M ammonium sulfate, VAPOR DIFFUSION, HANGING DROP, temperature 300K |