3KM0
17betaHSD1 in complex with 3beta-diol
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Detector technology | IMAGE PLATE |
| Detector | RIGAKU RAXIS II |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 154.420, 43.120, 121.100 |
| Unit cell angles | 90.00, 128.59, 90.00 |
Refinement procedure
| Resolution | 18.980 - 2.300 |
| R-factor | 0.23695 |
| Rwork | 0.233 |
| R-free | 0.31178 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.039 |
| RMSD bond angle | 3.278 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 18.980 |
| High resolution limit [Å] | 2.300 |
| Number of reflections | 25734 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | VAPOR DIFFUSION, HANGING DROP |
