3KLP
17beta-HSD1 in complex with A-diol
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS II |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 122.440, 44.020, 60.980 |
Unit cell angles | 90.00, 99.70, 90.00 |
Refinement procedure
Resolution | 18.650 - 2.500 |
R-factor | 0.17276 |
Rwork | 0.169 |
R-free | 0.25381 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.028 |
RMSD bond angle | 2.512 |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 18.650 |
High resolution limit [Å] | 2.500 |
Number of reflections | 8781 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |