3KLD
PTPRG CNTN4 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-BM |
Synchrotron site | APS |
Beamline | 22-BM |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-10-12 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 1.00 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 100.432, 138.957, 50.565 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.867 - 1.999 |
R-factor | 0.182 |
Rwork | 0.179 |
R-free | 0.23200 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.354 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER (2.1.4) |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.156 | 0.475 |
Number of reflections | 46797 | |
<I/σ(I)> | 5.8 | 3.6 |
Completeness [%] | 95.8 | 80.3 |
Redundancy | 12.5 | 8.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 10% PEG 1500 - 50 mM Sodium cacodylate pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |