3KL8
CaMKIINtide Inhibitor Complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.2 |
Synchrotron site | ALS |
Beamline | 8.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-02-09 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | .9537 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 72.410, 83.080, 145.130 |
Unit cell angles | 90.00, 101.93, 90.00 |
Refinement procedure
Resolution | 71.708 - 3.372 |
R-factor | 0.234 |
Rwork | 0.230 |
R-free | 0.28100 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.101 |
Data reduction software | MOSFLM (3.3.9) |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 83.100 | 3.600 |
High resolution limit [Å] | 3.400 | 3.400 |
Number of reflections | 21523 | |
Completeness [%] | 98.3 | 98.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7 | 293 | 20% 2-methyl-2,4-pentanediol, pH 7.0, VAPOR DIFFUSION, temperature 293K |