3KKJ
X-ray structure of P. syringae q888a4 Oxidoreductase at resolution 2.5A, Northeast Structural Genomics Consortium target PsR10
Replaces: 1YVVExperimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X4A |
Synchrotron site | NSLS |
Beamline | X4A |
Detector technology | CCD |
Detector | ADSC QUANTUM 4 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 120.698, 120.698, 114.791 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 2.500 |
R-factor | 0.234 |
Rwork | 0.227 |
R-free | 0.28100 |
Structure solution method | SAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.641 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | PHENIX ((phenix.refine: 1.4_115)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.600 |
High resolution limit [Å] | 2.500 | 2.500 |
Number of reflections | 64481 | |
Completeness [%] | 92.3 | 80.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 293 | CRYSTALLIZATION CONDITIONS: 100MM SODIUM ACETATE, 2000MM SODIUM FORMATE, PH 4.6, VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 293K |