3KJO
Crystal Structure of hPOT1V2-dTrUd(AGGGTTAG)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.1 |
Synchrotron site | ALS |
Beamline | 8.2.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-07-31 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0000 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 101.867, 103.591, 71.736 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.700 - 1.800 |
Rwork | 0.228 |
R-free | 0.23800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1xjv |
RMSD bond length | 0.005 |
RMSD bond angle | 1.200 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | REFMAC |
Refinement software | CNS (1.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.045 | 0.332 |
Number of reflections | 35300 | |
<I/σ(I)> | 22.2 | 3.9 |
Completeness [%] | 99.5 | 97.8 |
Redundancy | 6.9 | 6.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 289 | AMMONIUM SULFATE, TRISODIUM CITRATE , pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 289K |