3KJL
Sgf11:Sus1 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-02-01 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0719 |
Spacegroup name | P 61 |
Unit cell lengths | 68.670, 68.670, 232.860 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.943 - 2.700 |
R-factor | 0.217 |
Rwork | 0.213 |
R-free | 0.25310 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3kik |
RMSD bond length | 0.002 |
RMSD bond angle | 0.623 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.4_129)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 59.400 | |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.112 | 0.757 |
Number of reflections | 17082 | |
<I/σ(I)> | 18.1 | 2.7 |
Completeness [%] | 100.0 | 100 |
Redundancy | 22.4 | 22.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 292 | see publication, pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 292K |