3KB0
Crystal structure of abscisic acid-bound PYL2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-D |
Synchrotron site | APS |
Beamline | 21-ID-D |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-08-16 |
Detector | MARRESEARCH |
Wavelength(s) | 1.0 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 61.269, 61.269, 255.100 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.790 - 1.950 |
R-factor | 0.215 |
Rwork | 0.213 |
R-free | 0.24100 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.014 |
RMSD bond angle | 1.565 |
Data reduction software | HKL-2000 |
Phasing software | PHASER (1.3.2) |
Refinement software | REFMAC |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 1.950 |
Number of reflections | 21673 |
Completeness [%] | 97.3 |
Redundancy | 39.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 298 | Ammonium sulfate, pH 7.5, VAPOR DIFFUSION, temperature 298K |