3K89
Structure of X. oryzae pv. oryzae KACC10331, Xoo0880(fabD) complexed with glycerol
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 4A |
Synchrotron site | PAL/PLS |
Beamline | 4A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-07-21 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.00000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 41.361, 74.095, 98.617 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.730 - 1.600 |
R-factor | 0.18044 |
Rwork | 0.179 |
R-free | 0.20974 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3EEN |
RMSD bond length | 0.010 |
RMSD bond angle | 1.227 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.730 | 1.640 |
High resolution limit [Å] | 1.600 | 1.599 |
Number of reflections | 38753 | |
Completeness [%] | 99.8 | 99.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 9 | 287 | pH 9.0, VAPOR DIFFUSION, HANGING DROP, temperature 287K |