Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL1-5 |
| Synchrotron site | SSRL |
| Beamline | BL1-5 |
| Temperature [K] | 90 |
| Detector technology | CCD |
| Collection date | 1997-12-05 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 1.0688, 0.9800, 0.9795, 0.9322 |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 89.943, 89.943, 46.481 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 25.960 - 1.900 |
| R-factor | 0.204 |
| Rwork | 0.202 |
| R-free | 0.25900 |
| Structure solution method | MAD |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | ELVES |
| Refinement software | REFMAC (4) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 45.000 | 1.900 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Rmerge | 0.097 | |
| Number of reflections | 23195 | |
| Completeness [%] | 99.6 | 98.4 |
| Redundancy | 11 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7.3 | 298 | 100MM BIS-TRIS buffer only, pH 7.3, VAPOR DIFFUSION, SITTING DROP, temperature 298K |
