3K6D

Crystal structure of Xenopus laevis T-cadherin EC1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSLS BEAMLINE X29A
Synchrotron site	NSLS
Beamline	X29A
Temperature [K]	100
Detector technology	CCD
Detector	ADSC QUANTUM 315
Wavelength(s)	0.9791
Spacegroup name	I 41 2 2
Unit cell lengths	78.910, 78.910, 62.577
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	27.902 - 1.800
R-factor	0.227
Rwork	0.227
R-free	0.28500
Structure solution method	SAD
RMSD bond length	0.017
RMSD bond angle	1.916
Data reduction software	MOSFLM
Data scaling software	SCALA
Phasing software	SOLVE
Refinement software	PHENIX

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000	1.900
High resolution limit [Å]	1.800	1.800
Rmerge	0.039	0.209
Number of reflections	17500
<I/σ(I)>	11	3.6
Completeness [%]	99.9	100
Redundancy	13.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7	277	50mM Zn acetate, 20 % PEG 3350, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 277K