3K3F
Crystal Structure of the Urea Transporter from Desulfovibrio Vulgaris
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X29A |
Synchrotron site | NSLS |
Beamline | X29A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-05-02 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.01 |
Spacegroup name | P 63 |
Unit cell lengths | 110.131, 110.131, 84.861 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 38.780 - 2.300 |
R-factor | 0.18 |
Rwork | 0.179 |
R-free | 0.20400 |
Structure solution method | SAD |
RMSD bond length | 0.018 |
RMSD bond angle | 1.469 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHELX |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.340 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.089 | 0.964 |
Number of reflections | 25924 | |
<I/σ(I)> | 14.4 | |
Completeness [%] | 99.4 | 95.2 |
Redundancy | 8.2 | 5.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | 23% PEG 1500, 100 mM Na Cacodylate, pH 6.5, VAPOR DIFFUSION, SITTING DROP, temperature 293K |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | 23% PEG 1500, 100 mM Na Cacodylate, pH 6.5, VAPOR DIFFUSION, SITTING DROP, temperature 293K |