3K18
Tellurium modified DNA-8mer
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X12C |
| Synchrotron site | NSLS |
| Beamline | X12C |
| Temperature [K] | 99 |
| Detector technology | CCD |
| Collection date | 2008-04-12 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 0.9795 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 42.695, 42.695, 24.213 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 18.890 - 1.500 |
| R-factor | 0.20239 |
| Rwork | 0.201 |
| R-free | 0.22323 |
| Structure solution method | SIRAS |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.841 |
| Data reduction software | d*TREK |
| Data scaling software | d*TREK |
| Phasing software | SHELXS |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 18.890 | 1.550 |
| High resolution limit [Å] | 1.500 | 1.500 |
| Rmerge | 0.075 | 0.427 |
| Number of reflections | 3659 | |
| <I/σ(I)> | 15 | 2.4 |
| Completeness [%] | 94.4 | 74.9 |
| Redundancy | 8.63 | 5.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6 | 293 | MPD,sodium cacodylate,spermine tetra-HCl, pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
