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3K08

Crystal Structure of CNG mimicking NaK mutant, NaK-NTPP, Na+ complex

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsALS BEAMLINE 8.2.1
Synchrotron siteALS
Beamline8.2.1
Detector technologyCCD
Spacegroup nameI 4
Unit cell lengths67.780, 67.780, 89.511
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution? - 1.620
Rwork0.212
R-free0.22700
Structure solution methodMOLECULAR REPLACEMENT
Refinement softwareCNS
Data quality characteristics
 Overall
High resolution limit [Å]1.620
Number of reflections25612
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION293MPD, NaCl, pH 6.5-8.5, vapor diffusion, temperature 293K

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