3K08
Crystal Structure of CNG mimicking NaK mutant, NaK-NTPP, Na+ complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.1 |
Synchrotron site | ALS |
Beamline | 8.2.1 |
Detector technology | CCD |
Spacegroup name | I 4 |
Unit cell lengths | 67.780, 67.780, 89.511 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | ? - 1.620 |
Rwork | 0.212 |
R-free | 0.22700 |
Structure solution method | MOLECULAR REPLACEMENT |
Refinement software | CNS |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.620 |
Number of reflections | 25612 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | MPD, NaCl, pH 6.5-8.5, vapor diffusion, temperature 293K |