3K03
Crystal Structure of CNG mimicking NaK mutant, NaK-DTPP, K+ complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-ID |
| Synchrotron site | APS |
| Beamline | 19-ID |
| Detector technology | CCD |
| Spacegroup name | I 4 |
| Unit cell lengths | 67.747, 67.747, 89.444 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | ? - 1.620 |
| Rwork | 0.207 |
| R-free | 0.22200 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.005 |
| RMSD bond angle | 1.405 |
| Phasing software | CNS |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| High resolution limit [Å] | 1.620 | 1.620 |
| Number of reflections | 25607 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 293 | MPD, KCl, pH 6.5-8.5, vapor diffusion, temperature 293K |
