3JZL
CRYSTAL STRUCTURE OF A PUTATIVE CYSTATHIONINE BETA-LYASE INVOLVED IN ALUMINUM RESISTANCE (LMOF2365_1314) FROM LISTERIA MONOCYTOGENES STR. 4B F2365 AT 1.91 A RESOLUTION
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-05-15 |
Detector | MARMOSAIC 325 mm CCD |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 54.407, 153.173, 183.990 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.436 - 1.910 |
R-factor | 0.211 |
Rwork | 0.210 |
R-free | 0.24100 |
Structure solution method | SAD |
RMSD bond length | 0.014 |
RMSD bond angle | 1.691 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELX |
Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 39.436 | 39.436 | 1.980 |
High resolution limit [Å] | 1.910 | 4.100 | 1.910 |
Rmerge | 0.068 | 0.028 | 0.398 |
Number of reflections | 58916 | 10951 | 8441 |
<I/σ(I)> | 7.62 | 22.4 | 1.5 |
Completeness [%] | 94.5 | 93.8 | 71.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 293 | 30.0000% polyethylene glycol 600, 5.0000% polyethylene glycol 1000, 10.0000% Glycerol, 0.1M MES pH 6.0, ADDITIVE: 0.001 M PYRIDOXAL-5'-PHOSPHATE, NANODROP', VAPOR DIFFUSION, SITTING DROP, temperature 293K |