3JVO
Crystal structure of bacteriophage HK97 gp6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-02-04 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.97931 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 196.751, 200.211, 51.169 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.780 - 2.100 |
R-factor | 0.196 |
Rwork | 0.194 |
R-free | 0.22600 |
Structure solution method | SAD |
RMSD bond length | 0.013 |
RMSD bond angle | 1.228 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHARP |
Refinement software | REFMAC (refmac_5.2.0019) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.180 |
High resolution limit [Å] | 2.100 | 4.520 | 2.100 |
Rmerge | 0.074 | 0.055 | 0.292 |
Number of reflections | 115130 | ||
<I/σ(I)> | 11.9 | ||
Completeness [%] | 97.3 | 99.3 | 87.4 |
Redundancy | 5.8 | 5.6 | 5.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 293 | 20% MPD, 0.1M calcium chloride, 0.1M sodium acetate, pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 293K |