3JUA
Structural basis of YAP recognition by TEAD4 in the Hippo pathway
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Detector technology | CCD |
Collection date | 2008-11-13 |
Detector | ADSC QUANTUM 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 100.982, 146.910, 165.471 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 3.000 |
R-factor | 0.23893 |
Rwork | 0.236 |
R-free | 0.28842 |
Structure solution method | SAD |
RMSD bond length | 0.012 |
RMSD bond angle | 1.876 |
Data scaling software | SCALA (3.2.25) |
Refinement software | REFMAC (5.4.0077) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 74.346 | 74.350 | 2.900 |
High resolution limit [Å] | 2.800 | 10.840 | 2.800 |
Rmerge | 0.060 | 0.031 | 0.605 |
Total number of observations | 3535 | 21139 | |
Number of reflections | 61276 | ||
<I/σ(I)> | 14.2 | 14.9 | 1.2 |
Completeness [%] | 99.9 | 97.8 | 100 |
Redundancy | 3.6 | 3.1 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | HANGING DROP | 5.6 | 298 | PEG10000, Mg Acetate, pH5.6, HANGING DROP, temperature 298K |