3IUY
Crystal structure of DDX53 DEAD-box domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 56.442, 61.251, 65.787 |
Unit cell angles | 90.00, 96.36, 90.00 |
Refinement procedure
Resolution | 45.130 - 2.400 |
R-factor | 0.204 |
Rwork | 0.201 |
R-free | 0.25100 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.157 |
Data reduction software | MOSFLM |
Data scaling software | SCALA (3.2.25) |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0035) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 65.382 | 45.130 | 2.530 |
High resolution limit [Å] | 2.400 | 7.590 | 2.400 |
Rmerge | 0.187 | 0.118 | 0.578 |
Total number of observations | 5056 | 24409 | |
Number of reflections | 17649 | ||
<I/σ(I)> | 13.4 | 4.1 | 1.2 |
Completeness [%] | 100.0 | 99.6 | 100 |
Redundancy | 9.3 | 8.6 | 9.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 277 | 27% PEG6000, 0.1M MES pH 6, 0.2M AmmoniumChloride, 15% Glycerol, 0.2M NaCl , VAPOR DIFFUSION, SITTING DROP, temperature 277K |