3IPX
X-Ray structure of Human Deoxycytidine Kinase in complex with ADP and an inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-05-07 |
Detector | NOIR-1 |
Wavelength(s) | 1.12 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 80.238, 80.238, 93.950 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 60.970 - 2.000 |
R-factor | 0.22322 |
Rwork | 0.220 |
R-free | 0.27795 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1p60 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.349 |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 60.970 |
High resolution limit [Å] | 2.000 |
Number of reflections | 19463 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.1 M sodium acetate, 25% PEG 4000, 8% isopropanol |