3IOX
Crystal Structure of A3VP1 of AgI/II of Streptococcus mutans
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-03-02 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97918 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 70.725, 153.057, 49.677 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.590 - 1.800 |
R-factor | 0.19 |
Rwork | 0.190 |
R-free | 0.22800 |
Starting model (for MR) | 1jmm |
RMSD bond length | 0.005 |
RMSD bond angle | 1.300 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 36.000 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.069 | 0.298 |
Number of reflections | 45578 | |
<I/σ(I)> | 16.5 | 6.3 |
Completeness [%] | 90.7 | 87.7 |
Redundancy | 5.1 | 4.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 4.6 | 298 | 30% MME PEG 2000, 0.2M Ammonium sulfate, 0.05M Sodium cacodylate, 0.05M fructose, pH 4.6, VAPOR DIFFUSION, temperature 298K |